Volume 21, Issue 148 (2024)
FSCT 2024, 21(148): 30-44 |
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Yousefi M, Bimakr M, Ghoreishi S M, Ganjloo A. Effect of Supercritical CO2 and Microwave-assisted Extraction Methods on Bioactive Compounds Extraction from Silybum marianum Seed. FSCT 2024; 21 (148) :30-44
URL: http://fsct.modares.ac.ir/article-7-67412-en.html
URL: http://fsct.modares.ac.ir/article-7-67412-en.html
1- Department of Food Science and Engineering, Faculty of Agriculture, University of Zanjan, Zanjan, Iran
2- Department of Food Science and Engineering, Faculty of Agriculture, University of Zanjan, Zanjan, Iran ,mandana.bimakr@znu.ac.ir
3- Department of Chemical Engineering, Faculty of Engineering, Isfahan University of Technology, Iran
2- Department of Food Science and Engineering, Faculty of Agriculture, University of Zanjan, Zanjan, Iran ,
3- Department of Chemical Engineering, Faculty of Engineering, Isfahan University of Technology, Iran
Abstract: (592 Views)
In the current study, the effect of different new extraction methods including supercritical carbon dioxide extraction (SC-CO2), microwave-assisted extraction (MAE) and also conventional Soxhlet extraction (CSE) were investigated on bioactive compounds recovery from Silybum marianum seed. The crude extraction yield (22.40± 0.15%) was obtained using CSE, while the efficiency of SC-CO2 and MAE were about 89 and 50% of those obtained using CSE. The highest free radical scavenging activity in terms of DPPH and HO radicals was obtained in extract obtained using SC-CO2. From the TPC analysis, the highest and lowest value was determined in extracts obtained using SC-CO2 (102.93± 0.14 mg GAE/g) and CSE (14.50± 0.18 mg GAE/g), respectively. Fatty acid composition was analyzed using Gas Chromatography–Mass Spectrometry. Linoleic and oleic acids were determined as the main fatty acids. Finally, it can be concluded that S. marianum seed is a potential source of bioactive compounds and new extraction techniques of SC-CO2 and MAE could be suggested as promising methods to substitute conventional method for successful recovery of bioactive compounds.
Keywords: Silybum marianum, Bioactive compounds, Supercritical carbon dioxide extraction, Microwave-assisted extraction.
Article Type: Original Research |
Subject:
Extraction of effective compounds
Received: 2023/02/9 | Accepted: 2024/01/20 | Published: 2024/05/21
Received: 2023/02/9 | Accepted: 2024/01/20 | Published: 2024/05/21
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